Volume 25, Issue 2, July 2016, Pages 492–500
S. Vijayakumar1, P. Srinivasan2, S. Dinagaran3, and J. Balaji4
1 Department of Physics, Government College of Engineering, Dharmapuri-636704, Tamil Nadu, India
2 Department of Physics, University College of Engineering, Panruti-607 106, Tamil Nadu, India
3 Department of Physics, University College of Engineering, Thirukkuvalai-610 204, Tamil Nadu, India
4 Department of Physics, University College of Engineering, Panruti-607 106, Tamil Nadu, India
Original language: English
Copyright © 2016 ISSR Journals. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
The title crystal was grown from ethanol solvent by slow evaporation method. In order to good quality of crystals involved various analytical techniques. The crystal structure was verified by single crystal X-ray diffraction (SXRD) and structural purity was revealed by powder X-ray diffraction (PXRD). The functional group of the grown crystal was examined by FTIR spectrum. From the UV-Visible spectrum, grown crystal found that there is no absorption in the entire visible region. Thermal stability of the grown crystal was identified by TGA-DTA and DSC studies. The physical stability of the grown crystal was measured by Vicker’s microhardness studies. The Nonlinear optical eccentric was evaluated by Kurtz-Perry powder technique.
Author Keywords: Slow evaporation, Ethanol, Single-XRD, Micro hardness, Second Harmonic Generation.
S. Vijayakumar1, P. Srinivasan2, S. Dinagaran3, and J. Balaji4
1 Department of Physics, Government College of Engineering, Dharmapuri-636704, Tamil Nadu, India
2 Department of Physics, University College of Engineering, Panruti-607 106, Tamil Nadu, India
3 Department of Physics, University College of Engineering, Thirukkuvalai-610 204, Tamil Nadu, India
4 Department of Physics, University College of Engineering, Panruti-607 106, Tamil Nadu, India
Original language: English
Copyright © 2016 ISSR Journals. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Abstract
The title crystal was grown from ethanol solvent by slow evaporation method. In order to good quality of crystals involved various analytical techniques. The crystal structure was verified by single crystal X-ray diffraction (SXRD) and structural purity was revealed by powder X-ray diffraction (PXRD). The functional group of the grown crystal was examined by FTIR spectrum. From the UV-Visible spectrum, grown crystal found that there is no absorption in the entire visible region. Thermal stability of the grown crystal was identified by TGA-DTA and DSC studies. The physical stability of the grown crystal was measured by Vicker’s microhardness studies. The Nonlinear optical eccentric was evaluated by Kurtz-Perry powder technique.
Author Keywords: Slow evaporation, Ethanol, Single-XRD, Micro hardness, Second Harmonic Generation.
How to Cite this Article
S. Vijayakumar, P. Srinivasan, S. Dinagaran, and J. Balaji, “Growth, Structural, Spectral and Nonlinear Optical investigations of 2,4-Dinitrochlorobenzene (DNCB) Crystals,” International Journal of Innovation and Scientific Research, vol. 25, no. 2, pp. 492–500, July 2016.
